Phenyl-2-nitropropene reduction
I recently had a dream of reducingp2np to the amine with sn and hcl
Procedure went like this.
in a 2 litre beaker was 30 grams of recristlized p2np. 120 grams granulated tin with just enough water to cover contents.
A mechanical stirrer was fitted and the contents was heated to 50c
added dropwise was 200ml of 37% hcl over a period of 8 hours
the contents upon conpletion of the reduction had gone from a yellow p2np colour to to clear water
I then carefully basified water to ph13 which percipertated out tin hydroxide whitch i filtered out
I then had a yellow as water phase with a little bit of sodium cloride in it from reaction
Next i evaperated down the water to yeild a yellow product mixed with sodium cloride
When it was dry i added 250ml dry ethanol which dessolved the organic phase but not the nacl i then had a nice yellow alcohol phase
Dropwise i added conc h2so4 which percipertated out a very white powder
I then filtered to collect 26 grams of product wich i thought was amphetamine sulphate but was not did it go to the oxime or some other intermediate could somewone with more knowledge tan me help
I would be much apprecaited thank you
Edit by Chemoleo: Changed title, you can't assume everyone knows what p2np is.
[Edited on 8-3-2005 by chemoleo]hzsgpnxovags
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